bijlage 1_Aanvullend_onderzoek_Dioxines.v2, incl. bijlagen.pdf

710-2023-21559001

Result +/- expanded measurement uncertainty (95%; k=2) < - Concentration below the indicated limit of quantification (LOQ) ND - not determined since none of the corresponding congeners was above the LOQ L.Q. = below limit of quantification

The results of examination refer exclusively to the checked samples. Any publication of this report requires written permission. An excerpt publication is not allowed. Eurofins GfA Lab Service GmbH · Neuländer Kamp 1a · D-21079 Hamburg Headquarters: Eurofins GfA Lab Service GmbH – Neuländer Kamp 1a D-21079 Hamburg HRB 115907 AG Hamburg General Managers: Dr. Felix Focke VAT No.: DE275912372 Hypovereinsbank ● Bank code: 207 300 17 ● Account No.: 7000002400 ● SWIFT-BIC: HYVEDEMME17 IBAN: DE12 2073 0017 7000 0024 00 Our General Terms & Conditions, available upon request and online at http://www.eurofins.de/lebensmittel/kontakt/avb.aspx, shall apply.

Accredited testing Laboratory by DIN EN ISO/IEC DAkkS according to DIN EN ISO/IEC 17025:2018 The accreditation is valid only for the scope listed in the annex of the

Eurofins GfA Lab Service GmbH Neuländer Kamp 1a D-21079 Hamburg GERMANY Tel: +49 40 49294 5050 Fax: +49 40 49294 5009 dioxins@eurofins.de Eurofins GfA Lab Service GmbH · Neuländer Kamp 1a · D-21079 Hamburg

www.dioxine.de; www.dioxins.de

Person in charge ASM

Eurofins Omegam B.V. attn. report Postbus 94685 1090 GR Amsterdam NIEDERLANDE

Ms. S. Böye Ms. S. Böye

Report date

21.08.2023

Page 1/3

{C5B9DFAC-83CE-471D-A056-22015ECED060}

Analytical report AR-23-GF-030013-01 AR-23-GF-030013-01 Sample Code 710-2023-21559002 ¹Reference ¹Sample sender Reception date time Transport by ¹Client Purchase order nr. ¹Purchase order date ¹Client sample code Number of containers Reception temperature End analysis

ÌAR-23-GF-Ç#Â-È-01/Î

107-2-1-1 005-10530-0004119258 report 17.08.2023 DHL 1598888 16.08.2023 7854803 1 room temperature 21.08.2023

¹: This information was provided by the customer. Data provided by the customer may have an impact on the validity of the test results.

Test results GFU02

polychlorinated dibenzodioxins and -furans (17 PCDD/F): water, drinking water, sewage (°) (#) Method Internal, GLS DF 130:2022-11-09, GC-MS/MS 2,3,7,8-TetraCDD < 0.720 pg/l 1,2,3,7,8-PentaCDD

1.08 ± 0.323

pg/l pg/l

1,2,3,4,7,8-HexaCDD

< 1.92

pg/l

1,2,3,6,7,8-HexaCDD

< 2.10

pg/l

1,2,3,7,8,9-HexaCDD

5.82 ± 1.74

pg/l pg/l

The results of examination refer exclusively to the checked samples. Any publication of this report requires written permission. An excerpt publication is not allowed. Eurofins GfA Lab Service GmbH · Neuländer Kamp 1a · D-21079 Hamburg Headquarters: Eurofins GfA Lab Service GmbH – Neuländer Kamp 1a D-21079 Hamburg HRB 115907 AG Hamburg General Managers: Dr. Felix Focke VAT No.: DE275912372 Hypovereinsbank ● Bank code: 207 300 17 ● Account No.: 7000002400 ● SWIFT-BIC: HYVEDEMME17 IBAN: DE12 2073 0017 7000 0024 00 Our General Terms & Conditions, available upon request and online at http://www.eurofins.de/lebensmittel/kontakt/avb.aspx, shall apply.

Accredited testing Laboratory by DIN EN ISO/IEC DAkkS according to DIN EN ISO/IEC 17025:2018 The accreditation is valid only for the scope listed in the annex of the

Page 2/3

Analytical report AR-23-GF-030013-01 Sample Code

710-2023-21559002

1,2,3,4,6,7,8-HeptaCDD

57.2 ± 17.2

pg/l pg/l

OctaCDD

621 ± 186

pg/l pg/l

2,3,7,8-TetraCDF

< 1.28

pg/l

1,2,3,7,8-PentaCDF

< 1.72

pg/l

2,3,4,7,8-PentaCDF

< 1.72

pg/l

1,2,3,4,7,8-HexaCDF

< 1.60

pg/l

1,2,3,6,7,8-HexaCDF

< 1.60

pg/l

1,2,3,7,8,9-HexaCDF

< 1.60

pg/l

2,3,4,6,7,8-HexaCDF

< 1.60

pg/l

1,2,3,4,6,7,8-HeptaCDF

< 1.75

pg/l

1,2,3,4,7,8,9-HeptaCDF

< 1.52

pg/l

OctaCDF

< 3.20

pg/l

WHO(2005)-PCDD/F TEQ (lower-bound)

2.42 ± 0.604

pg/l pg/l

WHO(2005)-PCDD/F TEQ (upper-bound)

4.91 ± 1.23

pg/l pg/l

I-TEQ (NATO/CCMS) (lower-bound)

2.31 ± 0.578

pg/l pg/l

I-TEQ (NATO/CCMS) (upper-bound)

5.19 ± 1.30

pg/l pg/l

GFU07 polychlorinated biphenyls (12 WHO PCB): water, drinking water, sewage (°) (#) Method Internal, GLS DF 130:2022-11-09, GC-MS/MS PCB 77 < 36.0 pg/l PCB 81

< 4.80

pg/l

PCB 105

< 78.0

pg/l

PCB 114

< 9.40

pg/l

PCB 118

< 280

pg/l

PCB 123

< 8.00

pg/l

PCB 126

< 4.60

pg/l

PCB 156

< 44.0

pg/l

PCB 157

< 8.20

pg/l

PCB 167

< 22.0

pg/l

PCB 169

< 24.0

pg/l

PCB 189

< 8.00

pg/l

The results of examination refer exclusively to the checked samples. Any publication of this report requires written permission. An excerpt publication is not allowed. Eurofins GfA Lab Service GmbH · Neuländer Kamp 1a · D-21079 Hamburg Headquarters: Eurofins GfA Lab Service GmbH – Neuländer Kamp 1a D-21079 Hamburg HRB 115907 AG Hamburg General Managers: Dr. Felix Focke VAT No.: DE275912372 Hypovereinsbank ● Bank code: 207 300 17 ● Account No.: 7000002400 ● SWIFT-BIC: HYVEDEMME17 IBAN: DE12 2073 0017 7000 0024 00 Our General Terms & Conditions, available upon request and online at http://www.eurofins.de/lebensmittel/kontakt/avb.aspx, shall apply.

Accredited testing Laboratory by DIN EN ISO/IEC DAkkS according to DIN EN ISO/IEC 17025:2018 The accreditation is valid only for the scope listed in the annex of the

Page 3/3

Analytical report AR-23-GF-030013-01 Sample Code

710-2023-21559002

WHO(2005)-PCB TEQ (lower-bound)

ND

pg/l

WHO(2005)-PCB TEQ (upper-bound)

1.20 ± 0.300

pg/l pg/l

2.42 ± 0.604

pg/l pg/l

WHO(2005)-PCDD/F+PCB TEQ (medium-bound)

4.26 ± 1.07

pg/l pg/l

WHO(2005)-PCDD/F+PCB TEQ (upper-bound)

6.11 ± 1.53

pg/l pg/l

GFTE1 TEQ-Totals WHO-PCDD/F and PCB (°) (#) Method Internal, DF:110-5/120-5/130-3/140-5, Calculation WHO(2005)-PCDD/F+PCB TEQ (lower-bound)

GFU11 polychlorinated biphenyls (7 Indicator PCB): water, drinking water, sewage (°) (#) Method Internal, GLS DF 130:2022-11-09, GC-MS/MS PCB 28 < 820 pg/l PCB 52

< 610

pg/l

PCB 101

< 980

pg/l

PCB 118

< 280

pg/l

PCB 138

< 720

pg/l

PCB 153

< 1160

pg/l

PCB 180

< 300

pg/l

Total 6 ndl-PCB (lower-bound)

ND

pg/l

Total 6 ndl-PCB (upper-bound)

4590 ± 1150

pg/l pg/l

Total 7 Indicator PCB (lower-bound)

ND

pg/l

Total 7 Indicator PCB (upper-bound)

4870 ± 1220

pg/l pg/l

(°) = The test was performed at the laboratory site: Am Neuländer Gewerbepark 4 (#) = Eurofins GfA Lab Service GmbH (Hamburg) is accredited for this test. Result +/- expanded measurement uncertainty (95%; k=2) < - Concentration below the indicated limit of quantification (LOQ) ND - not determined since none of the corresponding congeners was above the LOQ L.Q. = below limit of quantification

The results of examination refer exclusively to the checked samples. Any publication of this report requires written permission. An excerpt publication is not allowed. Eurofins GfA Lab Service GmbH · Neuländer Kamp 1a · D-21079 Hamburg Headquarters: Eurofins GfA Lab Service GmbH – Neuländer Kamp 1a D-21079 Hamburg HRB 115907 AG Hamburg General Managers: Dr. Felix Focke VAT No.: DE275912372 Hypovereinsbank ● Bank code: 207 300 17 ● Account No.: 7000002400 ● SWIFT-BIC: HYVEDEMME17 IBAN: DE12 2073 0017 7000 0024 00 Our General Terms & Conditions, available upon request and online at http://www.eurofins.de/lebensmittel/kontakt/avb.aspx, shall apply.

Accredited testing Laboratory by DIN EN ISO/IEC DAkkS according to DIN EN ISO/IEC 17025:2018 The accreditation is valid only for the scope listed in the annex of the

RPS Advies- en Ingenieursbureau BV T.a.v. de heer R. Heeres Ptolemaeuslaan 40 3528BP UTRECHT

Uw kenmerk : NL202033308.004-Onderzoek dioxines Volgermeerpolder Ons kenmerk : Project 1578333 Validatieref. : 1578333_certificaat_v1 Opdrachtverificatiecode : NELB-UNXS-PLYN-IKLI Bijlage(n) : 3 tabel(len) + 1 bijlage(n) Bijlage dioxines (extern lab) in 1578333_-_7802344_dioxines_(extern_lab).pdf Bijlage dioxines (extern lab) in 1578333_-_7802345_dioxines_(extern_lab).pdf Bijlage dioxines (extern lab) in 1578333_-_7802342_dioxines_(extern_lab).pdf Bijlage dioxines (extern lab) in 1578333_-_7802343_dioxines_(extern_lab).pdf

Amsterdam, 18 juli 2023 Hierbij zend ik u de resultaten van het laboratoriumonderzoek dat op uw verzoek is uitgevoerd in de door u aangeboden monsters. De resultaten hebben uitsluitend betrekking op de monsters, zoals die door u voor analyse ter beschikking werden gesteld. Het onderzoek is, met uitzondering van eventueel uitbesteed onderzoek, uitgevoerd door Eurofins Omegam volgens de methoden zoals ze zijn vastgelegd in het geldende accreditatie-certificaat L086 en/of in de bundel "Analysevoorschriften Eurofins Omegam". De in dit onderzoek uitgevoerde onderzoeksmethoden van de geaccrediteerde analyses zijn in een aparte bijlage als onderdeel van dit analyse-certificaat opgenomen. De methoden zijn, voor zover mogelijk, ontleend aan de accreditatieprogramma's/schema's en NEN- EN- en/of ISO-voorschriften. Ik wijs u erop dat het analyse-certificaat alleen in zijn geheel mag worden gereproduceerd. Ik vertrouw erop uw opdracht volledig en naar tevredenheid te hebben uitgevoerd. Heeft u naar aanleiding van deze rapportage nog vragen, dan verzoek ik u contact op te nemen met onze klantenservice. Hoogachtend, namens Eurofins Omegam,

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